色譜填料技術(shù) —— 色譜柱整體效果的關(guān)鍵所在-江蘇美睿斯科環(huán)?？萍加邢薰?/title> <meta name="description" content=""> <meta name="keywords" content=""> <link href="/css/HituxCMSLoad/inner.css" rel="stylesheet" type="text/css" /> <link href="/css/HituxCMSLoad/common.css" rel="stylesheet" type="text/css" /> <script type="text/javascript" src="/js/jquery.min.js"></script> <script type="text/javascript" src="/js/functions.js"></script> <script type="text/javascript" src="/images/iepng/iepngfix_tilebg.js"></script> <script type="text/javascript"> window.onerror=function(){return true;} </script> <meta http-equiv="Cache-Control" content="no-transform" /> <meta http-equiv="Cache-Control" content="no-siteapp" /> <script>var V_PATH="/";window.onerror=function(){ return true; };</script> </head> <body> <h1><a href="http://zeronano.cn/">美日韩毛片,天天爽夜夜爽,亚洲性久久久影院,最近中文字幕免费mv</a></h1><div id="kkgmm" class="pl_css_ganrao" style="display: none;"><strike id="kkgmm"></strike><input id="kkgmm"><li id="kkgmm"><center 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id="pnbtnnv" class="clearfix"></div> </div> <div id="pnbtnnv" class="HeightTab clearfix"></div> </div>  <div id="pnbtnnv" class="right"> <div id="pnbtnnv" class="Position"><span>你的位置：<a href="/">首頁(yè)</a> > <a href='/News/'>新聞動(dòng)態(tài)</a> > <a href='/News/IndustryNews/'>行業(yè)新聞</a></span></div> <div id="pnbtnnv" class="HeightTab clearfix"></div>  <div id="pnbtnnv" class="main">  <div id="pnbtnnv" class="content"> <div id="pnbtnnv" class="title"><h3>色譜填料技術(shù) —— 色譜柱整體效果的關(guān)鍵所在</h3></div> <div id="pnbtnnv" class="infos">2016-10-28 15:13:47??????點(diǎn)擊：<script language="javascript" src="/inc/article_view.asp?id=1600"></script></div> <div id="pnbtnnv" class="maincontent clearfix"> <div>色譜是一種分離分析手段，分離是核心，因此擔(dān)負(fù)分離作用的色譜柱是色譜系統(tǒng)的心臟，色譜填料則是色譜技術(shù)的核心。除了固定相性能外，色譜填料技術(shù)對(duì)色譜柱的整體效果也起著至關(guān)重要的作用，裝填技術(shù)是獲得高效液相色譜柱的重要環(huán)節(jié)。</div> <div><br /> </div> <div>　　填料</div> <div><br /> </div> <div>　　常見(jiàn)的分配柱填料包括：碳十八柱[1]（ODS/C18)、碳八柱（MOS/C8）、碳六柱（Hexyl/C6）、碳四柱（Butyl/C4）、碳一柱（Methyl/C1）、陰離子交換柱（SAX)、陽(yáng)離子交換柱（SCX）、苯基柱（Phenyl）、氨基柱（Amino/NH2）、氰基柱（Cyano/CN/Nitrile）。常見(jiàn)的吸附柱填料有硅膠柱。隨著科技的快速發(fā)展，色譜柱填料也在不斷翻開(kāi)新篇章。出現(xiàn)了石墨化碳填料、貫流色譜填料和整體柱。</div> <div><br /> </div> <div>　　整體柱是一種新型的用于分離分析或作為反應(yīng)器的多孔介質(zhì)。早在2010年，色譜行業(yè)專家于泓教授便認(rèn)為整體柱將會(huì)成為一個(gè)發(fā)展趨勢(shì)。那時(shí)市面上已經(jīng)出現(xiàn)了一些硅膠型整體柱的產(chǎn)品，比如默克公司已生產(chǎn)出反相整體柱。同傳統(tǒng)色譜柱球形顆粒，填充緊密，間隙較小的特點(diǎn)不同，整體柱的空間由聚合物顆粒中的孔和顆粒間的縫隙組成。當(dāng)流動(dòng)相經(jīng)過(guò)大孔時(shí)，阻力小，使得液相色譜的流速提高，但柱壓不會(huì)明顯升高，高流速可以達(dá)到10ml/min(使用填充柱流速一般為1ml/min～1.5ml/min之間)。分離在樣品流經(jīng)孔結(jié)構(gòu)時(shí)發(fā)生，可以減少路徑的差異和縱向擴(kuò)展。所以整體柱具有快速分離，穩(wěn)定性很好的突出特點(diǎn)。</div> <div><br /> </div> <div>　　同填料一起發(fā)展的還有填料技術(shù)。利用亞2μm小粒徑硅膠、核殼型硅膠已成為填料技術(shù)發(fā)展一大趨勢(shì)。該技術(shù)擁有非常豐富的選擇性。包括HILIC色譜填料、極性嵌入反相色譜填料、立體保護(hù)鍵合相、有機(jī)-無(wú)機(jī)雜化色譜填料、親水性體積排阻(SEC)色譜填料、混合模式色譜填料、手性色譜填料和有機(jī)高分子基質(zhì)液相色譜填料。2μm填料粒徑還可以實(shí)現(xiàn)高速、高分辨率、高靈敏度的分離分析。目前，市面上能生產(chǎn)2μm色譜柱的企業(yè)還不多。</div> <div><br /> </div> <div>　　近年來(lái)，我色譜技術(shù)得到飛速發(fā)展，相關(guān)產(chǎn)學(xué)研活動(dòng)也蓬勃開(kāi)展。隨著市場(chǎng)的進(jìn)一步拓寬，色譜技術(shù)將為我們帶來(lái)更多更便利的應(yīng)用。</div> <div><ul style="font-family:'Microsoft Yahei', Arial, Helvetica, sans-serif;"><div id="pnbtnnv" class="albumblock" style="padding:10px 15px 30px 17px;margin:0px;float:left;width:190px;height:240px;"><div id="pnbtnnv" class="inner" style="padding:0px;margin:auto;width:190px;height:240px;position:relative;border:1px solid #ffffff;overflow:hidden;background-image:url("/images/BigRed/block_bg1.gif");background-attachment:initial;background-size:initial;background-origin:initial;background-clip:initial;background-position:50% 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